Development of analysis method for m‑xylenediamine as aldehyde scavenger using HPLC–PDA
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초록

The objective of this study was to develop an analytical method for m-xylenediamine (m-XDA), an aldehyde scavenger, in various food simulants and food matrices. The analysis was performed using HPLC-UV (270 nm) with a Capcell pak MGII C18 column (4.6 x 250 mm, 5 mu m). The method validation encompassed evaluations of specificity, linearity, accuracy, precision, limit of detection (LOD), and limit of quantification (LOQ) across five food simulants and six food matrices. In the calibration curve range of 1-100 mu g/mL, excellent linearity was observed with R-2 >= 0.9992. The accuracy and precision were within the ranges of 86.4-98.6% and 0.7-2.9 relative standard deviation (RSD%), respectively. The LOD and LOQ were in the ranges of 0.26-0.56 mu g/mL and 0.79-1.71 mu g/mL, respectively. The significance lies in the development of analysis methods for each food matrix, not only for smart packaging simulant analysis. This research makes it well-suited for smart packaging safety management.

키워드

Smart packagingActive packagingm-xylenediamineAnalytical methodMethod validationMIGRATION
제목
Development of analysis method for m‑xylenediamine as aldehyde scavenger using HPLC–PDA
저자
Shim, Ji-WonKim, Sun-HaeShin, Han-SeungShin, Jae-Wook
DOI
10.1007/s10068-024-01646-5
발행일
2025-01
유형
Article
저널명
Food Science and Biotechnology
34
1
페이지
95 ~ 102