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Copper-Mediated Intramolecular N-N Bond Coupling Using Cerium(IV) Sulfate as the Oxidant for the Synthesis of 5-Thio-Substituted 1,2,4-Triazoles
- Issue Date
- Dec-2015
- Publisher
- GEORG THIEME VERLAG KG
- Keywords
- copper; triazole; N-N coupling; cerium sulfate; heterocycles
- Citation
- SYNTHESIS-STUTTGART, v.47, no.24, pp 3874 - 3880
- Pages
- 7
- Indexed
- SCI
SCIE
SCOPUS
- Journal Title
- SYNTHESIS-STUTTGART
- Volume
- 47
- Number
- 24
- Start Page
- 3874
- End Page
- 3880
- ISSN
- 0039-7881
1437-210X
- Abstract
- A method for copper(II)-mediated N-N bond formation of N-imidoylisothioureas has been developed for the synthesis of 1,2,4-triazoles. The reaction requires cerium(IV) sulfate as an oxidant and proceeds at room temperature. This approach provides access to a variety of substituted 1,2,4-triazoles.
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