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Tandem One-Pot Synthesis of 2H- and 3H-Pyrroles Enabled by Dual Rh(II)/Pd(0) Catalysis
- Authors
- Choi, Seoung-Mi; Yun, Yuri; Kim, Ju Hyun
- Issue Date
- Nov-2024
- Publisher
- Georg Thieme Verlag
- Keywords
- 2H -pyrrole; 3H -pyrrole; dual catalysis; regioselectivity; N -tosyltriazole
- Citation
- Synthesis, v.56, no.22, pp 3405 - 3411
- Pages
- 7
- Indexed
- SCIE
SCOPUS
- Journal Title
- Synthesis
- Volume
- 56
- Number
- 22
- Start Page
- 3405
- End Page
- 3411
- ISSN
- 0039-7881
1437-210X
- Abstract
- Regioselective approaches toward 2H- and 3H-pyrroles,which are biologically important but easily isomerizable compounds, have been successfully achieved via dual Rh(II)/Pd(0) relay catalysis and DBU-mediated processes in one-pot operation using N-tosyltriazoles and hydroxymethylallyl carbonates. In this transformation, readily accessible N-tosyltriazoles were enabled as stable nitrogen sources for the two scaffolds, and the regioselectivity was controlled by the substituent positions of the hydroxymethylallyl carbonates.
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Related Researcher
- Kim, Ju Hyun
- College of Natural Science (Department of Chemistry)