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Green synthesis of palladium nanoparticles using fenugreek tea and their catalytic applications in organic reactions
- Authors
- Mallikarjuna, Koduru; Bathula, Chinna; Buruga, Kezia; Shrestha, Nabeen K.; Noh, Yong-Young; Kim, Haekyoung
- Issue Date
- 15-Oct-2017
- Publisher
- ELSEVIER
- Keywords
- Nanoparticles; Green catalyst; Nitrophenol; Suzuki-Miyaura reaction; FTIR
- Citation
- MATERIALS LETTERS, v.205, pp 138 - 141
- Pages
- 4
- Indexed
- SCI
SCIE
SCOPUS
- Journal Title
- MATERIALS LETTERS
- Volume
- 205
- Start Page
- 138
- End Page
- 141
- ISSN
- 0167-577X
1873-4979
- Abstract
- In this communication, we present the fenugreek tea aided green synthesis of Pd nanoparticles (PdNPs@ FT). The synthesized PdNPs were characterized by UV-Visible spectroscopy, scanning electron microscopy (SEM), small area electron diffraction (SAED), fourier transform infrared spectroscopy (FTIR) and X-ray diffraction (XRD). FT-IR manifested that polyol and amide groups present in fenugreek may have participated in the synthesis of palladium nanoparticles. PdNPs@ FT exhibited high catalytic activity towards hydrogenation of 4-nitrophenol to 4-aminophenol. PdNPs@ FT catalyzed SuzukiMiyaura coupling reaction between bromobenzene and phenyl boronic acid gave desired biphenyl in excellent yield. (C) 2017 Elsevier B.V. All rights reserved.
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Related Researcher
- Devasahayam, Bathula Chinna
- College of Engineering (Department of Electronics and Electrical Engineering)